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January 21, 2020

Gas phase FR effects of aluminium – phosphorus FRs

A research study analyses the differing gas phase fire-inhibition effects of two different aluminium – phosphorus PIN FRs (AHP aluminium hypophosphite, from Qingzhou Yichao Chemicals, and AlPi aluminium diethylphosphinate, from pinfa member Clariant) at 10% loading in PBT (polybutylene terephthalate).

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Magnesium – AlPi synergy in polyamide

Micron-sized magnesium oxide (MgO <75 µm) at 0 – 0.5 % loading, and AlPi (aluminium diethylphosphinate) at 0 – 14 % loading, were tested as synergistic PIN FRs in polyamide PA66, after extrusion and injection.

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AlPi as PIN FR for rigid polyurethane foam

Aluminium diethylphosphinate was tested at 0 – 11 % loading in rigid polyurethane foam (PUR), produced by one-step mixing, water blowing.

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January 14, 2020

AMI

Gerd Allermann, AMI, opened this 14th Fire Resistance in Plastics, noting that the conference has again brought together over 160 delegates from across the world. He identified four key themes for the...

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pinfa and Cefic

Jonathan Crozier, pinfa and Cefic, outlined the new needs for flame retardants in plastics in emobility. Electric vehicles are currently less than 2% of the world automotive market (but nearly 5% in China), but growth is expected to exceed 70% per year.

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Solvay

Cécile Corriol and Xavier Couillens, Solvay, presented developments in performance PIN-FR polyamide (Solvay Technyl) materials responding to new requirements for electric vehicles.

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ICL-IP

Lein Tange, ICL-IP, set the scene for the discussion with a summary of the challenges and opportunities for recycling technical plastics and a presentation of several European R&D and pilot industrial recycling projects. The EU WEEE Directive (Waste Electrical and Electronic Equipment 2012/19/EU) obliges to separate out plastics containing brominated flame retardants.

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Institute for Testing and Certification (Czech Republic)

Franky Puype, Institute for Testing and Certification (Czech Republic), presented the analysis of brominated flame retardants in 3 consumer goods made of recycled plastics purchased in the EU (cube toy, kaleidoscope toy, bottle cooler) using the Frontier Laboratories Pyrolysis system.

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Panel discussions on recycling

This year’s Flame Retardants in Plastics Conference included a panel discussion on recycling, moderated by Isabel de Castro, Flame Retardants Europe, with Chris Thornton of pinfa, Karen Janssens of Campine, Rudolf Pfaendner of Fraunhofer LBF and Lein Tange of ICL-IP

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Carl Spaeter GmbH

Carl Spaeter supplies different grades of the mineral flame retardant MDH, in particular for cables for different sectors (transport, electrical, construction …), and to applications in construction, such as roofing membranes.

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De Monchy International

De Monchy centres on providing quality products to customers, ensuring high levels consistent over coming years. Sustainability is a priority for the company, which is moving away from brominated FRs with a developing offer of ‘green’ and non-toxic FRs.

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Fire and Polymers Belgium

Günter Beyer, Fire and Polymers Belgium, summarised possibilities of bio-sourced flame retardants, Phytic acid (inositol hexaphosphoric acid), the natural phosphorus storage molecule in plants (especially in seeds), with up to 28% P by weight, has been demonstrated to be an effective flame retardant, and is readily available.

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Materia Nova Research Centre Belgium

Fouad Laoutid, Materia Nova Research Centre Belgium, presented research into fire safety functionalisation of polylactide (PLA, a bio-based polymer) by inserting phosphorus compounds, such as DOPO-diamine, as initiator for lactide ring opening polymerization.

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Klaus Lederer, POLOPLAST

POLOPLAST’s policy is to offer PIN flame retardant solutions, considered to be the future for fire safety. Health and safety, both for POLOPLAST’s own staff and for customers, is a priority and leads to prefer PIN FRs which offer benefits and quality technical support from PIN FR suppliers.

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CREPIM

Hervé Feuchter, CREPIM France, presented results of the comparison of smoke emissions from neat polymers and from polymers with FRs. This is the first time that such extensive data has been developed...

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Clariant

Christian Battenberg, Clariant, presented innovations in phosphorus-based PIN flame retardants for demanding applications in E&E and transport.

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Fraunhofer IFAM

Nick Wolter, Fraunhofer IFAM (see pinfa Newsletter n°105 FRPM 2019), presented the Mat4Rail project, developing innovative composite materials using polybenzoxazine (high performance, low density polymer), basalt fibre reinforcement and phosphorus PIN FRs.

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CellMark

Frédéric Roquefeuil, CellMark, presented this group’s development into fire safety. The group was founded in 1984 in Sweden with roots in the pulp and paper industry, acquiring Alcan International Network in 2012. CellMark has today 700 staff worldwide and a strong emphasis on developing a safer and more sustainable chemistry.

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Shinichi Ikoma and Shinji Sakaguchi, Daihachi

Daihachi sees phosphorus as the key to fire safety in the future as users look for alternative solutions to halogenated chemicals.

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Kostas Gatos, TERNA MAG

TERNA MAG expects that the prospects of market growth for flame retardants will induce new developments in relevant materials and polymeric recipes, on the basis of optimum (technically and cost wise) solutions.

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Muhammad Waseem, Gabriel Chemie

Polyolefins in general, and polyproylene in particular, are one of Gabriel Chemie’s specialist sectors for halogen free flame retardants, providing masterbatches for extrusion and injection moulding applications with demanding fire safety and technical specifications such as stadium seats (see pinfa Newsletter n°44), films for aviation transport, construction, mining industry.

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Bernd Hönig, Constab

Constab optimises formulations to achieve customers’ needs for specific and often demanding applications. PIN FRs are now available which offer heat stability in processing, are melt blendable, easy to process and can be transparent or colour-compatible.

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Jürgen Troitzsch

Jürgen Troitzsch, consultant, summarised trends in fire safety standards. Increasingly, standards are designed to allow fire safety to be achieved by different approaches: use of inherently fire resistant materials, fire barriers or flame retardants.

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ICL

Marc Leifer, ICL, summarised trends and perspectives in fire safety, as seen by his company. Civilisation has been marked by great fires, from Rome in 64 BC to San Francisco in 1906.

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